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Boron nitride components for MOCVD

Hot-pressed hexagonal Boron Nitride is often referred to as “white graphite” since it has similar layer structure as graphite. It has outstanding thermal characteristics: high thermal conductivity and excellent thermal shock resistance. It is stable up to 2000 °C in reducing atmospheres, and up to 900 °C in oxidizing atmospheres. It has features such as highly machinable, low thermal expansion, microwave transparency and high wet resistance to molten metals, slags and glass. Boron nitride ceramic parts are widely used as PVD, MOCVD, MBE system, furnace components, melting crucibles, insulators, washers, nozzles, microwave tubes, heat sink and heat radiation shielding.

BN Plate
An MOCVD reactor is a chamber made of a material that does not react with the chemicals being used. It must also withstand high temperatures. This chamber is composed of reactor walls, a liner, a susceptor, gas injection units, and temperature control units.
In the MOCVD reactor, the substrate is supported by a pedestal, which also acts as a susceptor. The pedestal/susceptor is the primary origin of heat energy in the reaction chamber. Only the susceptor is heated, so gases do not react before they reach the hot wafer surface. The reaction chamber walls in a cold-wall reactor, however, may be indirectly heated by heat radiating from the hot pedestal/susceptor, but will remain cooler than the pedestal/susceptor and the substrate the pedestal/susceptor supports. So Boron Nitride is a good choice because the power density, operating temperature, insulation grade and dielectric strength of heating elements can be greatly improved by using Boron Nitride as an insulator. It is also more economical and reduces thermal inertia. The annular shape reduces the size of the heating system and improves heat transfer.

BN
What should I pay attention to when I use Boron Nitride products?
1. Keep BN products in vacuum package before usage.
2. After vacuum package is removed, store BN products in dry and cool environment. Keep container tightly closed while not in use.
3. BN products are brittle. Please handle with care.


The difference between boron nitride crucible and alumina crucible

As an important part of chemical equipment, crucible is a container for melting and refining liquid metal and heating solid-liquid reaction. It is the basis for ensuring the smooth progress of chemical reactions.
There are many types of crucibles. According to the raw materials, ceramic crucibles can be divided into boron nitride crucibles, alumina crucibles, zirconia crucibles, aluminum nitride crucibles, quartz crucibles, etc. Here we mainly introduce the difference between boron nitride crucibles and alumina crucibles.
The advantages of boron nitride ceramics crucible compared to alumina ceramics crucible are:

boron nitride ceramics crucible
1.The temperature is high, and the long-term use temperature of boron nitride under vacuum is 1800 degrees, and the long-term use of 2100 degrees under the protection of the atmosphere. Alumina does not exceed 1700 degrees.
2.Strong thermal shock resistance, rapid cooling and no cracking. The boron nitride ceramics are taken out of the 1000 degrees furnace and quenched by the air blower, and will not crack even if repeated 100 times.
3.It is resistant to acid and alkali corrosion, has strong electrical insulation, and has a resistance to electrical breakdown of 3 to 4 times that of alumina.
4.Boron nitride ceramics do not react with many metals, ceramics, rare earth and other materials. Such as ferrous metal, iron, copper, stainless steel, tantalum, aluminum, tin, chromium, lead, nickel, magnesium, etc., glass melt, soda glass, cryolite, etc., silicon lava: slag, fluoride and the like. It can be used as a container, enamel, setter, etc.
The disadvantages of boron nitride ceramics crucible compared to alumina ceramics crucible are:

alumina ceramics crucible
1.Boron nitride ceramics have lower strength, hardness and wear resistance than alumina, and are not suitable for use in vibration and friction environments.
2.Boron nitride ceramics should not be used in the air at temperatures exceeding 1000 degrees. Exceeding oxidation, boron nitride can only be used up to 2000 degrees under vacuum or atmosphere protection.


Ceramic Heater Used in FFF 3D Printer

Innovacera developed ceramic heater used in FFF 3D pinter to replace the metal heaters, which speed up the heating time and improve the printing accuracy and speed.

Ceramic heater used in 3D printer
The Advantages of ceramic heater:
1. Small size;
2. Fast heating rate;
3. More uniform thermal performance, and thermal efficiency;
4. To integrate with thermistor, so as to achieve the purpose of accurate temperature control;
5. To improve the printing accuracy and speed;

MCH heater used in 3D printer
MCH heater technology:

Design Diameter/Length/Width Tolerance Thickness
Tube/Rod D:2.5~12 D: Above 8mm±0.3mm
Below8mm±0.2mm
L:10~120 LAbove80±2.0mm
Below80mm±1.0mm
Plate:Square L:10~100 Above:70±2mm 0.5~2
W:5-50 Below:70±1mm
Plate:Round D:10~70 Above:30±2mm 0.5~2
Below:30±1mm

Regular size and specification:

NO Model Size Resistance Voltage Shape Material
1 E0863TB OD6.3*ID5.2*8mm 0.25-0.4Ω 3.7V Tube 95%Alumina
2 E1416TA OD16*ID14.4*14mm 0.45-0.65Ω 3.7V Tube 95%Alumina
3 E13295TA D2.95*13mm 0.25-0.4Ω 5V Rod 95%Alumina
4 E13596TA OD9.6*ID8*13.5mm 0.45-0.6Ω 3.7V Tube 95%Alumina
5 E112015TA OD19.85*ID13.3*11mm 0.4-0.6Ω 3.7V Tube 95%Alumina
6 E131684FA OD16*ID7*13.8mm 0.4-0.6Ω 3.7V Tube 95%Alumina
7 E141895TA OD17.6*ID16.6*14mm 0.5Ω 3.7V Tube 95%Alumina
8 P1100TB D11*0.8mm 0.5-0.7Ω 3.7V Plate 95%Alumina

What’s the Ceramic Heater for Soldering Iron

Innovacera heating element is the PROCESS of MCH (Metal Ceramics Heater). It is the material of tungsten, molybdenum, molybdenum, manganese, and other high melting points Metal heating resistance paste is printed on 92 ~ 96% alumina flow ceramic green billet according to the requirements of heating circuit planning, with 4 ~ 8% sintering agent multi-layer superposition. At 1500 ~ 1600°C under high temperature burning into one body has the advantages of corrosion resistance, high temperature resistance, long life, high efficiency and energy saving, uniform temperature, good thermal conductivity, thermal compensation speed, and does not contain lead, cadmium, mercury, hexavalent chromium, polybrominated biphenyl, polybrominated diphenyl ethers, and other harmful substances, in line with the European Union RoHS environmental protection requirements. It is another generation product after alloy heating wire and PTC heating element.

ceramic heater for Soldering Iron
First, let’s make simply introduce the Soldering Iron. See the picture below for details.
(1)Soldering Iron

soldering iron
(2)Disassembly view (front)

Front disassembly drawing of Soldering Iron
(3)Disassembly view (rear)

Soldering Iron rear disassembly diagram
And then taking a look at the structure of the ceramic heating core. The outer diameter of the heating core is 3.8mm, which is suitable for a variety of internal heating soldering irons. There is a groove in the outer packaging ceramics, which is beneficial to the sintering of the manufacturing process and the elimination of working thermal stress. At the same time, please pay attention to the terminal at the root, which is relatively firm.
Brief introduction of ceramic heating core:
1) Main specifications:
Size: D3.8*60mm; D3.8*ID1.5*60mm .
Voltage: A:110V/130ohm, resistance deviation: ±10%
B: 220V/420ohm, resistance deviation: ±10%, can rise to 600-700°C power about 30W Heating area 25mm.
2) structure

Ceramic heating core structure diagram
In addition to the D3.8*60mm specification, we also have a variety of other specifications. Customization is also available.


Applications of precision ceramics in front-end semiconductors

Semiconductor equipment requires a large number of precision ceramic components. Because of the advantages of high hardness, high elastic modulus, high wear resistance, high insulation, corrosion resistance and low expansion, it can be used as parts of silicon wafer polishing machine, epitaxy/oxidation/diffusion heat treatment equipment, photolithography machine, deposition equipment, semiconductor etching equipment, ion implanter and so on. Semiconductor ceramics are alumina, silicon nitride, aluminum nitride, silicon carbide, boron nitride, and so on, in semiconductor equipment, the value of precision ceramics about 16% .

What are the precision ceramics used in semiconductor equipment
1. Alumina (Al2O3)
Alumina (Al2O3) is the most widely used ceramic material in semiconductor equipment. It has the advantages of stable material structure, high mechanical strength, high hardness, high melting point, corrosion resistance, good chemical stability, high resistivity, and good electrical insulation. In semiconductor etching equipment, high purity Al2O3 coating or Al2O3 ceramics are mainly used as the protective materials for etching cavity and its inner parts. In addition to the cavity, the plasma equipment gas nozzle, gas distribution plate and fixed ring fixed wafer also need to use alumina ceramics. Ceramic mechanical arms made of alumina ceramics are used in the handling of silicon wafers. From the material price, processing difficulty and other economic aspects, alumina ceramic robot arm cost-effective higher.
In addition, in wafer polishing process, alumina ceramics can be widely used in polishing plate, polishing pad correction platform, vacuum sucker, etc. .
2. Aluminum nitride (ALN)
High purity aluminum nitride ceramics have excellent thermal conductivity, heat resistance, insulation, Coefficient of thermal expansion close to silicon, and excellent plasma resistance. It can be used in heater of wafer heating, electrostatic Chuck, etc..
3. Silicon nitride (Si3N4)
Silicon nitride (Si3N4) is a kind of material with high fracture toughness, high heat shock resistance, high wear resistance, high mechanical strength, and corrosion resistance. It can be used in semiconductor equipment, such as the platform, bearings, and other components.
4. Boron nitride (BN)
BN has the advantages of high resistance, high temperature resistance, high electric breakdown resistance, no pollution, corrosion resistance and easy processing. Can be used in MOCVD equipment insulation heat dissipation, PVD/CVD vacuum coating equipment insulation accessories, ion implantation machine insulation accessories.
5. Silicon carbide (SiC)
Silicon carbide is characterized by high thermal conductivity, high temperature mechanical strength, high stiffness, low Coefficient of thermal expansion, good thermal uniformity, corrosion resistance and wear resistance. Silicon carbide can maintain good strength at extreme temperatures up to 1400 ° C. Because of its high hardness and low wear, and its Coefficient of thermal expansion are almost the same as that of silicon wafers, the lapping disc using silicon carbide ceramics can be lapped and polished at high speed. During the production of silicon wafers, high temperature heat treatment is needed, and silicon carbide jigs are often used to transport them. They are heat-resistant, non-destructive, and can be coated with DLC coatings, which can enhance the performance and alleviate the damage of wafers, at the same time to prevent the spread of pollution.
In addition, silicon carbide ceramics can also be used in XY platform, pedestal, focusing ring, polishing plate, wafer Chuck, vacuum sucker, carrier arm, furnace tube, crystal boat, cantilever propeller.


What is aluminum nitride ceramics

Aluminum nitride (AIN) is known for its high thermal conductivity and excellent electrical insulation properties. It is a common ceramic material used in a variety of electrical devices. In addition to its coefficient of thermal expansion and electrical insulation capabilities, aluminum nitride ceramics are resistant to most molten metals, such as copper, lithium and aluminum.

AIN ceramics
Properties of aluminum nitride ceramics
Aluminum nitride has a variety of properties that make it suitable for a variety of industrial applications:
High thermal conductivity (above 170 W/mK). This is close to the value of BeO and SiC and more than five times that of aluminum oxide (Al2O3).
Its coefficient of thermal expansion is 4.5 *10-6°C, the same as that of silicon (3.5-4 *10-6°C).
It has good light transmission properties
It is not toxic.
Good electrical conductivity. Aluminum nitride’s electrical properties include its dielectric constant, dielectric loss, bulk resistivity and dielectric strength – all of which make it an excellent insulating material.
Good mechanical properties: Aluminum’s mechanical properties are also responsible for its widespread use in industrial processes. It has a higher flexural strength than aluminum oxide (Al2O3) and beryllium oxide (BeO) ceramics.
Wide range of aluminum nitride ceramics
Aluminum nitride ceramics are used in many applications because of their good properties, including high thermal conductivity, low dielectric constant and dielectric loss, high dielectric strength, and significant resistance to plasma erosion.
Chip heat dissipation and support
Aluminum nitride ceramic substrates (ceramic trays) in semiconductor devices
Aluminum nitride etch shielding
Aluminum nitride evaporation boats for OLEDs
Also used for packaging of various electronic components


What is PTC Heaters

Definition:
A positive temperature coefficient heating element (PTC heating element) or self-regulating heater is an electrical resistance heater whose resistance increases significantly with temperature. The name self-regulating heater comes from the tendency of such heating elements to maintain a constant temperature.
PTC heating elements are a type of thermistor.

Positive-Temperature-Coefficient-PTC-heaters
Advantages of PTC heaters:
1.The surface temperature of PTC ceramic heater can be controlled automatically.
2.Good voltage shock resistance, the highest withstand voltage can reach more than 1300VDC, which ensures the reliability of components working under high voltage for a long time.
3.The temperature rises rapidly at low temperature, and it can start quickly even if the ambient temperature reaches -40 degrees.
4.The power aging is extremely small under high DC voltage, and it can still maintain a good heating effect after long-term use.
5.Curie temperature and PTC size can be adjusted arbitrarily according to customer requirements, ranging from 60 degrees to 315 degrees.
6. Long service life
7. Aluminum spraying, screen printing aluminum, silver, welding and other electrode layers are produced and supplied at the same time.
Applications:
1.Heating or defrosting in air conditioners, pure electric vehicles and hybrid electric vehicles, or for heating battery boxes.
2.Liquid and solid mosquito coils and incense perfumes.
3.Air heaters, bathroom heaters, coffee pots and foot baths and other small household appliances.
Innovacera offer ceramic heater solutions for customers, if you have any inquiry, pls feel free to send to us.


Big Promotion for Innovacera Ceramic Igniter

Why choose Innovacera ceramic igniter for wood pellet ignition?

230V 250W Alumina Ceramic Wood Pellet Boiler
It is due to below reasons:
1.High Performance: Providing fast and reliable ignition, allowing for quick start-up of wood pellet boilers or stoves. The igniters reach high temperatures rapidly, ensuring efficient ignition of the pellets.
2.Durability: Using high-quality materials and advanced manufacturing techniques to ensure the durability and longevity .
3.Resistance to Environmental Factors: We are engineered to withstand various environmental factors that can affect ignition, such as moisture, dust, and contamination from the wood pellets. This resistance contributes to the igniters’ reliability and consistent performance.
4.Energy Efficiency: It is designed to be energy-efficient, consuming low power during the ignition process. This not only helps reduce energy costs but also contributes to the overall efficiency of the wood pellet system.
5.Versatility: We are versatile and can be used in a wide range of wood pellet boilers and stoves. They are compatible with various ignition systems and can be retrofitted as replacements for existing igniters, making them a convenient choice for upgrading or repairing wood pellet heating systems.
6.Quality Manufacturing: We are known for its commitment to quality manufacturing processes. Our igniters undergo rigorous testing and quality control measures to ensure consistent performance and reliability.
7.Industry Experience: We have a wealth of experience in the field of igniter technology, for various applications, including wood pellet ignition, for many years.
August is our anniversary, in order to thank the support of new and old customers, we will give 5% discount for orders over $300, please contact our sales department for details.
The specific content is subject to the news published on our official website.


5% Discount for Innovacera Ceramic Igniter

August is coming soon! At the same time, august is Innovacera’s anniversary. In order to celebrate it and and feedback new and old customers, we will launch a promotion for igniters. Get 5% off all ceramic igniter orders throughout August.

ceramic igniter

ceramic igniter

INNOVACERA offers ceramic igniters for hot surface ignition systems in heating applications. These high strength, heat resistant ceramic igniters have become an industry standard in gas heating systems. Their superior materials and rapid heating capabilities provide reliable performance over a long useful life.
Applications include:
• Straw burner
• Other biomass burner
• Wood pellet burner
• Wood chips burner
• Other biomass burner
• And more
INNOVACERA offers two styles of ceramic igniters, white and black ceramic igniters. Both leveraging strong properties including:
• Ready assembled, easy-to-install systems
• Space-saving, noiseless and impervious to
overheating (in case the blower fails)
• Extremely long-lasting and resilient
• Minimal energy consumption
• Completely electrically insulated
• No exposed electrical contacts
• No sensitive welding points
• Long lasting (non aging)
• Time to ignition 60~90 seconds
• Available in 100V / 120V / 220V / 240VAC
Some igniter specifications are as follows:

Model Voltage/Power Size Wire
INC-H1-1/2/3/4 230V 90*Φ10.5*φ6.5mm 300-500mm
210W/225W/240W/255W
INC-H2-1/2 230V 160W/180W 90*Φ10.5*φ6.5mm 300-500mm
INC-H3-1 120V 230W 90*Φ10.5*φ6.5mm 300-500mm
INC-H4-1/2 230V 350W/300W 108*Φ11.5*φ6.5mm 300-500mm
INC-H5-1/2/3/ 230V 150W/170W 70*Φ10.5*φ6.5mm 300-500mm
INC-H5-4 230V 230W 70*Φ84-133*φ6.5mm 300-500mm
INH-1-230 230V 270W-315W 106*11.5

This table is only a partial ceramic igniter specification. For more information please contact us.
In addition to regular sizes and specifications, we also accept customized. Don’t miss this discount, contact us with no hesitation!


Precautions For Installation Of Ceramic Ignite

Ceramic igniter, which is used for the ignition of biomass (especially wood pellet) burning system. It can also be adapted to other specific application (biofuel system, water boiling, industrial oven, etc).

High Temperature 26mm Alumina Ceramic Hot Surface Igniter with Flange Cap

High Temperature 26mm Alumina Ceramic Hot Surface Igniter with Flange Cap

Installation prohibition
Please design your system in order that the heating element of the heater never enters directly in contact with solid fuel or ashes or metal protective tube. If the heating element enters in contact with solid fuel, ashes or metal protective it could damage the heating element. Longer protective tube should be consider to avoid this situation.
Please make sure to let an interspace of minimum 3mm around the ceramic heating element and the tube.

Diagram-of-a-stove-using-a-pot-burner-combustion-system

Diagram-of-a-stove-using-a-pot-burner-combustion-system

Information
For use beyond typical operating conditions or applications, please consult your INNOVACERA sales representative or distributor for further information.
For more information can see on INNOVACERA web site.
About INNOVACERA
INNOVACERA was incorporated in 2012 and since then producing ignition components for gas and biomass sector. The company complies with ISO 9001 and ISO14001.


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